The Selection of Solvents Used for Recrystalization of Octogen (The first report on the study

程景才; 陆庆武

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The Selection of Solvents Used for Recrystalization of Octogen (The first report on the study

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- The Selection of Solvents Used for Recrystalization of Octogen (The first report on the study
- 奥克托今重结晶所用溶剂的选择——奥克托今粒度研究报告之一
- Issue 3, Pages: 47-58(1986)
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- Published：1986
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程景才, 陆庆武. The Selection of Solvents Used for Recrystalization of Octogen (The first report on the study[J]. 1986, (3): 47-58.
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程景才, 陆庆武. The Selection of Solvents Used for Recrystalization of Octogen (The first report on the study[J]. 1986, (3): 47-58. DOI：

摘要

本文讨论了用溶剂非溶剂沉淀技术制取不同粒度的奥克托今(代号 HMX)。根据结晶化学的基本原理

对国内外曾用过溶剂的性质、经济效益等方面进行比较。通过实验确定用二甲亚砜(代号 DMSO)作溶剂。通过百克级试验控制重结晶条件得到所要求的符合美军标准粒度规格的六种粒度。质量达到科研课题要求。文中对 DMSO 用量与丙酮精制的丙酮用量进行了比较并将试验结果和美国资料在 DMSO 用量及得率方面进行了比较。结果表明本研究的 DMSO 用量、精制得率和经济效益等方面均优于现有文献报导。

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