高艳阳, 张月, 王金霞. Solid State Synthesis of PbO Nanorods[J]. 2007, (1): 57-59.
DOI:
高艳阳, 张月, 王金霞. Solid State Synthesis of PbO Nanorods[J]. 2007, (1): 57-59.DOI:
Solid State Synthesis of PbO Nanorods
摘要
分别以Pb(Ac)2.3H2O、Pb(NO3)2为原料
与NaOH在室温条件下进行固相化学反应
得到了纳米PbO粒子.通过在反应体系中添加NaCl
成功地制得了棒状PbO纳米粒子.运用X射线衍射(X-Ray Diffractomer
XRD)和透射电镜(Transmission Electron Microscope
TEM)对产物进行了表征.研究表明
氯离子的存在对产物PbO的形貌有很大影响.
Abstract
Nanometer PbO were prepared by solid state reaction at room temperature via sodium hydroxide and lead acetate or lead nitrate
and PbO Nanorods were successfully prepared in the presence of sodium chloride.The productions were characterized by X-ray Diffractomer(XRD) and Transmission Electron Microscope(TEM).The result indicates that the chloride ion has much influence on the formation of PbO nanorods.
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references
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