Preparation of One-Demensional Nanostructure ZnO

姜秀平; 高艳阳; 贾素云

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Preparation of One-Demensional Nanostructure ZnO

更新时间：2026-09-14

- Preparation of One-Demensional Nanostructure ZnO
- 一维纳米结构ZnO的制备
- Issue 2, Pages: 147-150(2008)
- 作者机构：
  
  中北大学化工与环境学院
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2008
- 稿件说明：
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姜秀平, 高艳阳, 贾素云. Preparation of One-Demensional Nanostructure ZnO[J]. 2008, (2): 147-150.
DOI：

姜秀平, 高艳阳, 贾素云. Preparation of One-Demensional Nanostructure ZnO[J]. 2008, (2): 147-150. DOI：

摘要

采用溶胶-凝胶法

以醋酸锌(Zn(CH3COO)2.2H2O)

草酸((COOH)2.2H2O)和无水乙醇为原料

制备得到了粒子直径在30 nm左右、粒度分布均匀、分散性较好的球状纳米ZnO粒子.以上述反应为基础

在反应体系中加入一定量的有机添加剂三乙醇胺

得到了棒状结构的纳米ZnO.利用透射电子显微镜(Transmission Electron Microscopy

TEM)研究了有机添加剂三乙醇胺的加入对产物纳米ZnO形貌的影响.实验结果表明:有机添加剂三乙醇胺在棒状纳米ZnO的形成过程中起决定性作用

并且所形成的棒状纳米ZnO的形貌随添加剂用量的不同而不同

所以调节三乙醇胺的加入量可以有效地控制纳米ZnO的形貌.

Abstract

A sol-gel process was used to synthesize nano-ZnO by using Zn(CH3COO)2·2H2O

H2C2O4·2H2O and CH3CH2OH as raw materials.The sphere-shaped product had an average diameter of 30 nm with uniform particle distribution and good dispersivity.The rod-like ZnO particles were obtained by adding triethanolamine to the reactive system on the basis of above reaction.The effects of organic additive triethanolamine on morphology of nano-ZnO were studied by Transmission Electron Microscopy(TEM).The results show that triethanolamine plays an important role in the process of rod-like ZnO particles' formation

and that the morphology of rod-like nano-ZnO is different with different quantities of the additive.So the morphology of nano-ZnO can be controlled effectively by triethanolamine.

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references

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